Synthesis and Characterization of Monodisperse Hydrous Colloidal Zirconia Nanoparticles

Thi Dieu Linh Nguyen, Quang Tung Nguyen, Quang Tham Do, Vu Giang Nguyen, Huu Trung Tran, Thi My Hanh Le, Thi Thu Trang Nguyen, Thuy Chinh Nguyen, Hoang Thai, Thi Mai Tran, Van Sy Do
Author affiliations

Authors

  • Thi Dieu Linh Nguyen Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
  • Quang Tung Nguyen Faculty of Chemical Technology, HaUI, Tay Tuu, North Tu Liem, Hanoi, Vietnam
  • Quang Tham Do Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi https://orcid.org/0000-0001-5480-4360
  • Vu Giang Nguyen Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
  • Huu Trung Tran Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
  • Thi My Hanh Le Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
  • Thi Thu Trang Nguyen Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
  • Thuy Chinh Nguyen Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi https://orcid.org/0000-0001-8016-3835
  • Hoang Thai Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
  • Thi Mai Tran Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
  • Van Sy Do Faculty of Chemical Technology, HaUI, Tay Tuu, North Tu Liem, Hanoi, Vietnam

DOI:

https://doi.org/10.15625/0868-3166/30/4/15422

Keywords:

colloidal zirconia, CZPs, monodispersion, zirconium oxychloride

Abstract

The suspension of hydrous colloidal zirconia particles (CZPs) was prepared from zirconium oxychloride solutions via thermal hydrolysis at acidic condition and at boiling point of 110 ºC for 72 h. Characterization of the obtained suspension and dried solid ZrO2 was performed by DLS, FESEM, FTIR, XRD and TGA measurements. Purification via dialysis membrane can maintain the monodispersion of the colloidal suspension when stabilized at pH6. The suspension contained almost sheet-like colloidal particles with amorphous structure with size ranges from 70 to 140 nm in wide and about 40-60 nm in thickness. The formula of hydrous CZPs can be expressed as ZrO2.2H2O.

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Published

25-11-2020

How to Cite

[1]
T. D. L. Nguyen, “Synthesis and Characterization of Monodisperse Hydrous Colloidal Zirconia Nanoparticles”, Comm. Phys., vol. 30, no. 4, p. 391, Nov. 2020.

Issue

Vol. 30 No. 4 (2020)

Section

Papers

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